Kim Kardashian, Kanye West

Just off their big Mexico vacation, hot couple Kim Kardashian and Kanye West are taking a little time apart.

The Keeping Up With the Kardashians star enjoyed some quality time with family over the weekend while her rapper beau hit the NYC club scene with Leonardo DiCaprio.

West hit hot spot PH-D Rooftop Lounge at Dream Downtown, where DiCaprio was enjoying a date night with model girlfriend Erin Heatherton. West arrived just before 2 a.m. and headed over to DiCaprio's table for hellos and a quick chat.

The 35-year-old Watch the Throne crooner then surprised clubgoers by grabbing his laptop and taking over the DJ booth to play songs from his upcoming unreleased album G.O.O.D.

West danced and lip-synced along to his music while shocked fans enjoyed his spur-of-the-moment music preview. He played for 45 minutes before leaving the club just after 3 a.m.

Meanwhile, back in L.A., Kardashian, 31, spent the weekend with her famous family. But it's not like West wasn't on her mind. "Wishing my prince was here with me tonight," Kardashian tweeted on Friday with a pic of an empty bed.

The next day, she tweeted, "Sleep over with Mason & Penelope tonight!" and on Sunday she posted, "Fun day at church with Mason today, then a BBQ & swimming with friends & family. Couldn't have been a more perfect Sunday!"

Keeping Up With the Kardashians airs Sundays at 9 p.m. on E!

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